For the majority of users conducting nuclear magnetic resonance (NMR) spectroscopy today, sample preparation follows a similar path: isolate a compound or compounds from a reaction mixture (or if ...

This technique’s ability to highlight molecular structure and track reaction dynamics has garnered widespread recognition throughout academia and industry as a robust, nondestructive, noninvasive ...

Please prepare your samples in the designated area or under a hood, and not on top of the magnet. The chemical shifts (d) of solvent signals observed for 1 H NMR and 13 C NMR spectra are listed in the ...

The emergence of peptide therapeutics marks a transformative shift in the types of products being developed and manufactured in the pharmaceutical industry. Peptides, defined by the FDA as biopolymers ...

Unfortunately, many 1H-NMR spectra are severely overlapped due to the multiplet structure caused by homo-nuclear scalar couplings. "Pure shift" NMR spectra, also known as broadband homonuclear ...

NMR spectra are typically collected in solutions made up of deuterated solvents due to the fact that a protonated solvent will yield large solvent peaks which may hide the solute’s spectral features.